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General synthetic approach to functionalized dihydrooxepines

Academic Article
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Overview

authors

  • Nicolaou, K.C.
  • Yu, R.
  • Shi, L.
  • Cai, Q.
  • Lu, M.
  • Heretsch, P.

publication date

  • April 2013

journal

  • Organic Letters  Journal

abstract

  • A three-step sequence to access functionalized 4,5-dihydrooxepines from cyclohexenones has been developed. This approach features a regioselective Baeyer-Villiger oxidation and subsequent functionalization via the corresponding enol phosphate intermediate.

subject areas

  • Catalysis
  • Combinatorial Chemistry Techniques
  • Cyclohexanones
  • Molecular Structure
  • Oxepins
  • Oxidation-Reduction
  • Stereoisomerism
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Identity

PubMed Central ID

  • PMC3653422

International Standard Serial Number (ISSN)

  • 1523-7052 (Electronic) 1523-7052 (Linking)

Digital Object Identifier (DOI)

  • 10.1021/ol4006689

PubMed ID

  • 23550898

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