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Studies on the synthesis of tedanolide. 2. Stereoselective synthesis of a protected C(1)-C(12) fragment

Academic Article
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Overview

authors

  • Roush, William
  • Newcom, J. S.

publication date

  • December 2002

journal

  • Organic Letters  Journal

abstract

  • [reaction: see text] Highly diastereoselective syntheses of diketo esters 6a and 6b are described. These intermediates undergo efficient aldol reactions with protected C(13)-C(21) aldehydes 3 and 23, thereby providing advanced C(1)-C(21) tedanolide seco ester precursors 9a and 9b.

subject areas

  • Aldehydes
  • Animals
  • Antineoplastic Agents
  • Esters
  • Lactones
  • Macrolides
  • Porifera
  • Stereoisomerism
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Identity

International Standard Serial Number (ISSN)

  • 1523-7060

Digital Object Identifier (DOI)

  • 10.1021/ol0272343

PubMed ID

  • 12489975
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Additional Document Info

start page

  • 4739

end page

  • 4742

volume

  • 4

issue

  • 26

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